Acrolein → HCID 86761216, compound

Participants

Reaction Steps

According to the General Procedure C, 1-Bromo-1-(3-ethoxy-4-methoxyphenyl)ethene (1.40 g, 5.44 mmol), t-BuLi (8.00 ml, 13.60 mmol) and acrolein (914 mg, 16.32 mmol) are converted to give after workup and chromatography [SiO2, PE/EE gradient from 5:1 to 2:1, Rf (PE/EE=2:1)=0.31] the title compound (1.10 g, 4.69 mmol) as a colorless oil;

Provenance & Evidence