Hydrogen Bromide → HCID 16085805, compound

Participants

Reaction Steps

According to the General Procedure D, HBr (33% in acetic acid, 1.22 ml, 0.51 g, 6.25 mmol) and 3-Ethoxy-4-methoxyphenylacetylene (1.10 g, 6.25 mmol) are converted to give after workup and chromatography (SiO2 PE/EE 5:1, Rf=0.35) the title compound (1.53 g, 5.83 mmol) as a brown oil; C11H13BrO2 (257.13).

Provenance & Evidence