p-Fluoronitrobenzene → HCID 68427704, compound

HRID 1174706Notes

Reaction equation

HRID 1174706 reaction equation
[NH:1]1[CH2:5][CH2:4][CH:3]2[NH:6][CH2:7][CH2:8][CH:2]12.F[C:10]1[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][CH:11]=1>>[N+:16]([C:13]1[CH:14]=[CH:15][C:10]([N:1]2[CH2:5][CH2:4][CH:3]3[NH:6][CH2:7][CH2:8][CH:2]23)=[CH:11][CH:12]=1)([O-:18])=[O:17]

Participants

3

Reactant 2

HCID 9590p-FluoronitrobenzeneHCID 15106927HCID 15106927, compound

Product 1

HCID 68427704HCID 68427704, compound

Procedure

Octahydropyrrolo[3,2-b]pyrrole (0.50 g) was reacted by method C with 4-fluoronitrobenzene (0.53 g). The product with the molecular weight of 233.27 (C12H15N3O2); MS (ESI): 234 (M+H+) was obtained in this way.

Workup

  1. customMS (ESI): 234 (M+H+) was obtained in this way

Sources & evidence

ORD record
ord-7cca1d61fd9c4647b5fcf933ee14a2cb
Source dataset
uspto-grants-2010_11
Patent number
US07838547B2

Reaction notes

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