HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,4-Dichlorophenoxy)acetic acid → 2-(3,4-Dichloro-phenoxy)-N-[2-(3-dimethylamino-pyrrolidin-1-yl)-benzothiazol-6-yl]-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,4-Dichlorophenoxy)acetic acid | HCID 11495 | — |
| Reactant | 2-(3-Dimethylamino-pyrrolidin-1-yl)-benzothiazol-6-ylamine | HCID 63231507 | — |
| Product | 2-(3,4-Dichloro-phenoxy)-N-[2-(3-dimethylamino-pyrrolidin-1-yl)-benzothiazol-6-yl]-acetamide | HCID 68775336 | — |
Reaction Steps
Prepare according to the procedures described in Example 1, step 4, Method B, using 3,4-dichlorophenoxyacetic acid (135 mg, 0.611 mmol) and 2-(3-dimethylamino-pyrrolidin-1-yl)-benzothiazol-6-ylamine (162 mg, 0.618 mmol) to afford the title compound, mass spectrum (m/e): 465 [M+H], 463 [M−H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07838543B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-194ca0e767174a558da831f9d657435c |
| Source note | uspto-grants-2010_11 |