HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1) → Methyl-(2-morpholin-4-yl-ethyl)-(6-nitro-benzothiazol-2-yl)-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1) | HCID 77210 | — |
| Edukt | N-Methyl-6-nitrobenzo[D]thiazol-2-amine | HCID 638568 | — |
| Produkt | Methyl-(2-morpholin-4-yl-ethyl)-(6-nitro-benzothiazol-2-yl)-amine | HCID 57771793 | — |
Reaktionsschritte
The title compound is prepared according to the general procedure outlined in Example 61, Step 2, utilizing methyl-(6-nitro-benzothiazol-2-yl)-amine (1.18 g, 5.64 mmol) and N-(2-chloroethyl)-morpholine hydrochloride (2.45 g, 13.17 mmol) to yield 1.43 g (79%) of the product. mass spectrum (ion-spray): (m/z)=323.2 (M+1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07838543B2 |
| Quelldatensatz | uspto-grants-2010_11 |
| ORD ID | ord-b1c1071765a44a038f29f75c10dc9a97 |
| Quellennotiz | uspto-grants-2010_11 |