4-Cyclopentylbenzoic acid → HCID 57771708, compound

HRID 1174973Notes

Reaction equation

HRID 1174973 reaction equation
[CH:1]1([C:6]2[CH:14]=[CH:13][C:9]([C:10]([OH:12])=O)=[CH:8][CH:7]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1.[CH3:15][N:16]([CH3:31])[CH2:17][CH2:18][N:19]([CH3:30])[C:20]1[S:21][C:22]2[CH:28]=[C:27]([NH2:29])[CH:26]=[CH:25][C:23]=2[N:24]=1>>[CH:1]1([C:6]2[CH:7]=[CH:8][C:9]([C:10]([NH:29][C:27]3[CH:26]=[CH:25][C:23]4[N:24]=[C:20]([N:19]([CH2:18][CH2:17][N:16]([CH3:15])[CH3:31])[CH3:30])[S:21][C:22]=4[CH:28]=3)=[O:12])=[CH:13][CH:14]=2)[CH2:2][CH2:3][CH2:4][CH2:5]1

Participants

3

Reactant 2

HCID 141636714-Cyclopentylbenzoic acidHCID 55226563N2-(2-Dimethylamino-ethyl)-N2-methyl-benzothiazole-2,6-diamine

Product 1

HCID 57771708HCID 57771708, compound

Procedure

The title compound is prepared by following General Method A, using 4-cyclopentyl-benzoic acid (0.099 g, 0.52 mmol), and N*2*-(2-Dimethylamino-ethyl)-N*2*-methyl-benzothiazole-2,6-diamine (0.10 g, 0.40 mmol) to give 0.38 g (23%) of product. LC/MS: Retention time=4.97 min; (m/z): calcd for C24H30N4OS (M+H)+: 423.6; found: 423.0.

Sources & evidence

ORD record
ord-f1bda3a7f3a640e18f681e2f753d194b
Source dataset
uspto-grants-2010_11
Patent number
US07838543B2

Reaction notes

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