Cyclohexene → HCID 57771780, compound
Reaction equation
I[C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=1.[CH:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH:12]=1>>[CH:16]1([C:2]2[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][CH:3]=2)[CH2:15][CH2:14][CH2:13][CH:12]=[CH:11]1Participants
3
Procedure
The title compound is prepared by following a procedure analogous to Example 114, Step 1, and using 4-iodobenzoic acid (3.0 g, 12.10 mmol), and cyclohexene (12.3 mL) to give the product (0.40 g, 1.98 mmol, 16%).
Sources & evidence
- ORD record
- ord-66c45fde6a604f38a010df520c5cd44f
- Source dataset
- uspto-grants-2010_11
- Patent number
- US07838543B2
Reaction notes
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