HRID1174979
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The title compound is prepared by following Method A, using 4-cyclohexylmethoxy-benzoic acid (Crooks, S. L.; Merrill, B. A.; Wightman, P. D. WO 9603983 A1.) (0.20 g, 0.86 mmol), and N*2*-(2-dimethylamino-ethyl)-N*2*-methyl-benzothiazole-2,6-diamine (0.17 g, 0.68 mmol) to afford 0.12 g (38%). LC/MS: Retention time=5.67 min; (m/z): calcd for C26H34N4O2S (M+H)+: 467.7; found: 467.0.
WORKUP
后处理
- customto afford 0.12 g (38%)