2-Chloro-4-methoxybenzeneboronic acid → HCID 11720193, compound

Participants

Reaction Steps

The title compound is prepared by following a procedure analogous to Example 113, Step 1, using N-{2-[(2-dimethylamino-ethyl)-methyl-amino]-benzothiazol-6-yl}-4-iodo-benzamide (0.05 g, 0.12 mmol) and 2-chloro-4-methoxy-phenyl boronic acid (0.026 g, 0.14 mmol) to afford 0.036 g (60%). LC/MS, Retention time=4.53 min; (m/z): calcd for C26H27ClN4O2S (M+H)+: 496.1; found: 496.0.

Provenance & Evidence