HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Tolylboronic acid → HCID 58789357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Tolylboronic acid | HCID 2733950 | — |
| Reactant | 2-(4-Bromophenyl)-N-isobutyl-2-methylpropanamide | HCID 68775075 | — |
| Product | HCID 58789357 | HCID 58789357 | 60% |
Reaction Steps
Prepared in a similar manner to Example 8 from 2-(4-Bromophenyl)-N-isobutyl-2-methylpropanamide (Example 1a) and m-tolylboronic acid. Yield: 60%. 1H NMR (400 MHz, CDCl3): δ 0.8 (d, 6H), 1.65 (s, 6H), 1.67-1.70 (m,1H), 2.3 (s, 3H), 3(t, 2H), 7.18 (d, 1H), 7.34 (t, 1H), 7.42 (m, 4H), 7.6 (dd, 2H). MS (M+H, 310).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842324B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-d84286b8200146ad865b5e99962da617 |
| Source note | uspto-grants-2010_11 |