HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl isocyanate → HCID 178418694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl isocyanate | HCID 76639 | — |
| Reactant | HCID 178419058 | HCID 178419058 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178418694 | HCID 178418694 | 19.1% |
Reaction Steps
A solution of 4-(2-furyl)-1H-pyrrolo[2,3-d]pyrimidine-2-amine (192 mg, 0.96 mmol) in THF (3 mL) was treated with benzyl isocyanate (118 μL, 0.96 mmol), stirred at room temperature for 16 h and the resulting solid filtered and washed with EtOAc to give the title compound (61 mg, 19%) as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07098333B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-e3a6e51d909246489019c19083530959 |
| Source note | uspto-grants-2006_08 |