HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isobutylamine → HCID 68773492, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isobutylamine | HCID 6558 | — |
| Reactant | 2-(4-bromopyrazol-1-yl)-2-methylpropanoic acid | HCID 7017278 | — |
| Product | HCID 68773492 | HCID 68773492 | 95% |
Reaction Steps
Prepared in a similar manner to Example 3 from 2-(4-bromo-1H-pyrazol-1-yl)-2-methylpropanoic acid and isobutylamine. Yield: 95%. 1H NMR (400 MHz, CDCl3): δ 0.81 (d, 3H, J=6.8 Hz), 1.63-1.67 (m, 1H), 1.84 (s, 6H), 2.99 (t, 2H, J=6.8 Hz), 6.19 (br, 1H), 7.61 (s, 1H), 7.64 (s, 1H). MS(MH+) 288, 290.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842324B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-001784a7e83840f89330964dd5dff68f |
| Source note | uspto-grants-2010_11 |