2-Formylphenylboronic acid → HCID 58789404, compound

Participants

Reaction Steps

Prepared in a similar manner to Example 1 from 2-(4-bromophenyl)-N-isobutyl-2-methylpropanamide (example 1a) and 2-formylphenylboronic acid. Yield: 59%. 1H NMR (400 MHz, dMSO): δ 0.72-0.75 (d, 6H), 1.49 (s, 6H), 1.65-1.72 (m, 1H), 2.80-2.85 (t, 2H), 7.35-7.44 (m, 5H), 7.47-7.50 (d, 1H), 7.55-7.65 (t, 1H), 7.70-7.75 (t, 1H), 7.85-7.90 (d,1H), 9.9 (s, 1H); MS+H (324).

Provenance & Evidence