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HRID1175617

反应详情

EQUATION

反应方程式

HRID 1175617 的结构方程式

REACTANTS

反应物

2
结构：COCc1cccc(B(O)O)c1
HCID3825855

3-Methoxymethylphenylboronic acid

C8H11BO3

结构：CC(C)(C(=O)O)c1ccc(Br)cc1
HCID10933679

2-(4-bromophenyl)-2-methylpropanoic acid

C10H11BrO2

PRODUCTS

生成物

1
结构：COCc1cccc(-c2ccc(C(C)(C)C(=O)O)cc2)c1
HCID68774399

未命名化合物

收率 82%

PROCEDURE

实验过程

Prepared in a similar manner to Example 1 starting from 3-(methoxymethyl)phenylboronic acid and 2-(4-bromophenyl)-2-methylpropanoic acid. Yield: 82%. 1H NMR (400 MHz, DMSO): δ 1.48 (s, 6H), 4.46 (s, 2H), 7.27-7.29 (d, 1H), 7.40-7.44 (m, 3H), 7.54-7.56 (d, 2H), 7.60-7.62 (d, 2H), 12.40 (s, 1H).