HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Pyrimidin-5-yl)boronic acid → HCID 16005192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Pyrimidin-5-yl)boronic acid | HCID 2795193 | — |
| Reactant | 2-(4-Bromophenyl)-N-isobutyl-2-methylpropanamide | HCID 68775075 | — |
| Product | HCID 16005192 | HCID 16005192 | — |
Reaction Steps
Prepared in a similar manner to Example 1 from 2-(4-bromophenyl)-N-isobutyl-2-methylpropanamide (example 1a) and pyrimidin-5-ylboronic acid. Yeld: 64%. 1H NMR (400 MHz, dMSO): δ 0.75-0.77 (d, 6H), 1.49 (s, 6H), 1.69-1.72 (m, 1H), 2.84-2.87 (t, 2H), 7.41 (t, 1H), 7.45-7.47 (d, 3H), 7.77-7.79 (d, 2H), 9.14 (s, 2H), 9.18 (s, 1H); MS+H (297.7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842324B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-9ca0e2c5b11b457dbf7525b80253e4a6 |
| Source note | uspto-grants-2010_11 |