HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → HCID 58789383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 86609794 | HCID 86609794 | — |
| Product | HCID 58789383 | HCID 58789383 | 75% |
Reaction Steps
Prepared in a similar manner to Example 1 from 4-(1-(isobutylamino)-2-methyl-1-oxopropan-2-yl)-2-methylphenyl trifluoromethanesulfonate (example 50a) and phenyl boronic acid. Yield: 75%. 1H NMR (400 MHz, dMSO): δ 0.76-0.77 (d, 6H), 1.46 (s, 6H), 1.72-1.73 (m, 1H), 2.21 (s, 3H), 2.84-2.87 (m, 2H), 7.13-7.21 (m, 3H), 7.30-7.37 (m, 4H), 7.41-7.45 (m, 2H); MS+H (310).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842324B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-7e8aff9aeecd4fffa3c325bf3357aa6b |
| Source note | uspto-grants-2010_11 |