Isobutylamine → HCID 68777357, compound

HRID 1175639Notes

Reaction equation

HRID 1175639 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]([CH3:14])([CH3:13])[C:10]([OH:12])=O)=[CH:5][C:4]=1[CH3:15].[CH2:16]([NH2:20])[CH:17]([CH3:19])[CH3:18]>>[CH2:16]([NH:20][C:10](=[O:12])[C:9]([C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[C:4]([CH3:15])[CH:5]=1)([CH3:14])[CH3:13])[CH:17]([CH3:19])[CH3:18]

Participants

3

Reactant 2

HCID 6558IsobutylamineHCID 68773494HCID 68773494, compound

Product 1

HCID 68777357HCID 68777357, compoundYield 64%

Procedure

Prepared in a similar manner to Example 35a starting from 2-(4-methoxy-3-methylphenyl)-2-methylpropanoic acid (example 50d) and isobutylamine. Yield: 64%. MS+H (264).

Workup

  1. customPrepared in a similar manner to Example 35a

Sources & evidence

ORD record
ord-51b47df93d854bce8380e9354d1740a2
Source dataset
uspto-grants-2010_11
Patent number
US07842324B2

Reaction notes

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