HCID 86624307, compound → HCID 66745636, compound

HRID 1175754Notes

Reaction equation

HRID 1175754 reaction equation
C([O:8][C:9]1[CH:23]=[CH:22][C:12]2[C:13](=[N:20]O)[CH2:14][C:15]3([O:19][C:11]=2[CH:10]=1)[CH2:18][CH2:17][CH2:16]3)C1C=CC=CC=1>CO.[Pd]>[NH2:20][CH:13]1[C:12]2[CH:22]=[CH:23][C:9]([OH:8])=[CH:10][C:11]=2[O:19][C:15]2([CH2:16][CH2:17][CH2:18]2)[CH2:14]1

Participants

4

Reactant 1

HCID 86624307HCID 86624307, compound

Product 1

HCID 66745636HCID 66745636, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 887MethanolSolvent

Procedure

This compound was prepared by hydrogenation of 7-Benzyloxy-3,4-Dihydro-4-hydroxyimino-spiro[2H-1-benzopyran-2,1′-cyclobutane] in presence of 10% Pd/C in methanol. The amine was isolated as hydrochloride salt.

Sources & evidence

ORD record
ord-109b8327bdbf4902a1ce1d20e6a67093
Source dataset
uspto-grants-2010_11
Patent number
US07842703B2

Reaction notes

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