Ethanol → HCID 23153869, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 4-chloro-1-(4-methoxybenzyl)-2-oxo-1,2-dihydroquinoline-3-carbonitrile (500 mg), 2-methoxyphenylhydrazine hydrochloride (321 mg), triethylamine (627 μl) and ethanol (5 ml) was stirred at room temperature for 1 hour and at 90° C. for 2 hours. After cooling, water was added to the mixture and the precipitated solid was collected by filtration, washed with water-ethanol and dried to obtain the target compound (421 mg).

Provenance & Evidence