HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-3-methoxypropane → [3-Methoxy-5-(3-methoxypropoxy)phenyl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-3-methoxypropane | HCID 118927 | — |
| Reactant | 3-(Hydroxymethyl)-5-methoxyphenol | HCID 592986 | — |
| Product | [3-Methoxy-5-(3-methoxypropoxy)phenyl]methanol | HCID 59817758 | — |
Reaction Steps
Analogously to Method F, 3.15 g of 3-hydroxymethyl-5-methoxyphenol are reacted with 1-chloro-3-methoxypropane. The title compound is obtained as a slightly yellowish oil. Rf=0.27 (1:1 EtOAc-heptane). Rt=3.23.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-a01d672a6b6c4534a6c4905df61c20f7 |
| Source note | uspto-grants-2010_11 |