Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Chloro-3-methoxypropane → 7-Hydroxymethyl-1-(3-methoxypropyl)-3,4-dihydro-1H-quinolin-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Chloro-3-methoxypropane | HCID 118927 | — |
| 반응물 | 7-(Hydroxymethyl)-3,4-dihydroquinolin-2(1H)-one | HCID 53393348 | — |
| 생성물 | 7-Hydroxymethyl-1-(3-methoxypropyl)-3,4-dihydro-1H-quinolin-2-one | HCID 68501224 | — |
반응 단계
Analogously to Example 2c, 1.28 g of 7-hydroxymethyl-3,4-dihydro-1H-quinolin-2-one are reacted with 1.59 ml of 1-chloro-3-methoxypropane. The title compound is obtained as a slightly yellowish oil. Rf=0.24 (dichloromethane-methanol=95:5); Rt=2.71.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07842688B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-34dac757f947483aa2dcb9d6f9a0e2be |
| 출처 메모 | uspto-grants-2010_11 |