HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19593725, compound → tert-Butyl 3-{[2-(2-acetylaminoethyl)phenylcarbamoyl]methoxy}-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19593725 | HCID 19593725 | — |
| Reactant | Tert-butyl 3-carboxymethoxy-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}piperidine-1-carboxylate | HCID 68504714 | — |
| Product | tert-Butyl 3-{[2-(2-acetylaminoethyl)phenylcarbamoyl]methoxy}-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}piperidine-1-carboxylate | HCID 68501851 | — |
Reaction Steps
Analogously to Example 3a, 0.138 g of tert-butyl 3-carboxymethoxy-4-{4-[3-(2-methoxybenzyloxy)propoxy]phenyl}piperidine-1-carboxylate and 0.061 g of N-[2-(2-aminophenyl)ethyl]acetamide. The title compound is obtained as a yellow oil. Rf=0.21 (95:5 dichloromethane-methanol); Rt=5.22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-37e6a2f0092a438489d3b1375226e8b2 |
| Source note | uspto-grants-2010_11 |