HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-3-methoxypropane → N-(2-bromo-5-methylphenyl)-N-(3-methoxypropyl)isobutyramide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-3-methoxypropane | HCID 118927 | — |
| Reactant | N-(2-bromo-5-methylphenyl)-2-methylpropanamide | HCID 68542723 | — |
| Product | N-(2-bromo-5-methylphenyl)-N-(3-methoxypropyl)isobutyramide | HCID 68505459 | — |
Reaction Steps
Analogously to Example 8c, 16.50 g of N-(2-bromo-5-methylphenyl)isobutyramide and 8.59 ml of 1-chloro-3-methoxypropane are reacted. The title compound is obtained as a slightly yellowish oil. Rf=0.13 (1:1 EtOAc-heptane); Rt=18.54 (II).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-611481d6a0c84635b95fb30a510326f0 |
| Source note | uspto-grants-2010_11 |