1-Chloro-3-methoxypropane → HCID 59224279, compound
Reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][C:3]=1[OH:9].Cl[CH2:11][CH2:12][CH2:13][O:14][CH3:15]>>[Br:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][C:3]=1[O:9][CH2:11][CH2:12][CH2:13][O:14][CH3:15]Participants
3
Procedure
Analogously to Method F, 10.0 g of 2-bromo-5-methylphenol and 11.6 g of 1-chloro-3-methoxypropane are reacted. The title compound is obtained as a slightly orange oil. Rf=0.31 (1:4 EtOAc-heptane); Rt=5.01.
Sources & evidence
- ORD record
- ord-e0bcc6642d944a8396e4366236122cd5
- Source dataset
- uspto-grants-2010_11
- Patent number
- US07842688B2
Reaction notes
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