Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1176441Generated: October 31, 2026

1-(3-bromopropoxy)-2-methylbenzene → HCID 68504039, compound

https://huagongshe.com/reaction/1176441

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(3-bromopropoxy)-2-methylbenzeneHCID 1622574—
Reactant(3S,4S)-tert-Butyl 3-hydroxy-4-(4-hydroxyphenyl)piperidine-1-carboxylateHCID 21713087—
ProductHCID 68504039HCID 68504039—

Reaction Steps

Analogously to Method I, 0.750 g of tert-butyl 3-hydroxy-4-(4-hydroxyphenyl)piperidine-1-carboxylate and 0.732 g of 1-(3-bromopropoxy)-2-methylbenzene are reacted. The title compound is obtained as a slightly yellowish oil. Rf=0.57 (1:2 EtOAc-heptane); Rt=5.45.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07842688B2
Source datasetuspto-grants-2010_11
ORD IDord-366ce5de03dc4fcbb26c1811881ade84
Source noteuspto-grants-2010_11