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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1176443Generated: November 1, 2026

1-(3-Bromopropoxy)-2-methoxybenzene → HCID 53688057, compound

https://huagongshe.com/reaction/1176443

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-(3-Bromopropoxy)-2-methoxybenzeneHCID 13116178—
Reactant(3S,4S)-tert-Butyl 3-hydroxy-4-(4-hydroxyphenyl)piperidine-1-carboxylateHCID 21713087—
ProductHCID 53688057HCID 53688057—

Reaction Steps

Analogously to Method I, 0.750 g of tert-butyl 3-hydroxy-4-(4-hydroxyphenyl)piperidine-1-carboxylate and 0.786 g of 1-(3-bromopropoxy)-2-methoxybenzene are reacted. The title compound is obtained as a slightly yellowish oil. Rf=0.25 (1:1 EtOAc-heptane); Rt=4.91.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07842688B2
Source datasetuspto-grants-2010_11
ORD IDord-7bd964096157482f826fca3b1e97abe2
Source noteuspto-grants-2010_11