HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(chloromethyl)-4-(3-methoxypropyl)-2H-benzo[b][1,4]oxazin-3(4H)-one → HCID 68501277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(chloromethyl)-4-(3-methoxypropyl)-2H-benzo[b][1,4]oxazin-3(4H)-one | HCID 46835223 | — |
| Reactant | HCID 68505152 | HCID 68505152 | — |
| Product | HCID 68501277 | HCID 68501277 | — |
Reaction Steps
Analogously to Method D, 1.10 g of tert-butyl 3-hydroxy-4-[4-(3-m-tolyloxypropoxy)phenyl]piperidine-1-carboxylate and 0.693 g 6-chloromethyl-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one (Example 2a) are reacted. The title compound is obtained as a colourless oil. Rf=0.60 (1:1 EtOAc-heptane); Rt=6.14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-621ff2fd6a1d4bea8322409b933054e3 |
| Source note | uspto-grants-2010_11 |