HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxysalicyl alcohol → [3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxysalicyl alcohol | HCID 78088 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Product | [3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol | HCID 43471496 | — |
Reaction Steps
Analogously to Method F, 2.44 g of 2-hydroxymethyl-6-methoxyphenol and 2.56 g of 2-bromoethyl methyl ether are reacted and the title compound is obtained as a colourless oil. Rf=0.22 (1:1 EtOAc-heptane); Rt=2.91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-fc59f8e97f4a491a90816f2b711a523b |
| Source note | uspto-grants-2010_11 |