HuagongsheHuagongshe Chemistry Print Report · For research reference only
3351-52-8 → HCID 68499269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3351-52-8 | HCID 15157497 | — |
| Reactant | (3S,4S)-tert-Butyl 3-hydroxy-4-(4-hydroxyphenyl)piperidine-1-carboxylate | HCID 21713087 | — |
| Product | HCID 68499269 | HCID 68499269 | — |
Reaction Steps
Analogously to Method I, 0.750 g of tert-butyl 3-hydroxy-4-(4-hydroxyphenyl)piperidine-1-carboxylate and 0.924 g of 1-(3-bromopropoxy)-3-trifluoromethylbenzene are reacted. The title compound is obtained as a slightly yellowish oil. Rf=0.28 (1:1 EtOAc-heptane); Rt=5.43.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-3e8d3a27ad3e4defbe9cc6ac4fab81b9 |
| Source note | uspto-grants-2010_11 |