HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-(chloromethyl)-4-(3-methoxypropyl)-2H-benzo[b][1,4]oxazin-3(4H)-one → HCID 68501433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-(chloromethyl)-4-(3-methoxypropyl)-2H-benzo[b][1,4]oxazin-3(4H)-one | HCID 46835223 | — |
| Reactant | HCID 68499094 | HCID 68499094 | — |
| Product | HCID 68501433 | HCID 68501433 | — |
Reaction Steps
Analogously to Method D, 13.34 g of benzyl 4-[4-(1-tert-butoxycarbonylazetidin-3-yloxy)phenyl]-3-hydroxypiperidine-1-carboxylate and 8.267 g of 6-chloromethyl-4-(3-methoxypropyl)-4H-benzo[1,4]oxazin-3-one are reacted. The title compound is obtained as a yellow oil. Rf=0.33 (2:1 EtOAc-heptane); Rt=5.53.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842688B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-60f4929cfc2849b1bb44da283d36d297 |
| Source note | uspto-grants-2010_11 |