3-Phenylphenol → HCID 11472211, compound

HRID 1176765Notes

Reaction equation

HRID 1176765 reaction equation
[C:1]1([C:7]2[CH:8]=[C:9]([OH:13])[CH:10]=[CH:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[O:15][C:16](=[O:25])[C:17]1[CH:22]=[CH:21][CH:20]=[C:19]([CH2:23]Br)[CH:18]=1>>[C:7]1([C:1]2[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=2)[CH:12]=[CH:11][CH:10]=[C:9]([O:13][CH2:23][C:19]2[CH:18]=[C:17]([CH:22]=[CH:21][CH:20]=2)[C:16]([OH:25])=[O:15])[CH:8]=1

Participants

3

Reactant 2

HCID 113813-PhenylphenolHCID 517981Methyl 3-(bromomethyl)benzoate

Product 1

HCID 11472211HCID 11472211, compound

Procedure

3-(Biphenyl-3-yloxymethyl)-benzoic acid was prepared using general procedure A from 3-phenylphenol (available from Aldrich, Milwaukee, Wis.) and 3-(bromomethyl)benzoic acid methyl ester (available from Lancaster Synthesis Ltd., Morcambe, Lancashire, UK). Yield: 76 mg. Mass spectrum (ES) MH+=305.

Sources & evidence

ORD record
ord-c652ea7f9c4c4548a64a57485d41f949
Source dataset
uspto-grants-2010_11
Patent number
US07842825B2

Reaction notes

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