Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 2-Naphthol | HCID 8663 | — |
| Product | 2-Naphthylamine | HCID 7057 | — |
Reaction Steps
In a sealed reactor, 4.32 g (30 mmol, 1 eq) of 2-naphthol, 2.85 g (30 mmol, 1 eq) of (NH4)2SO3 and 50 mL of aqueous ammonia were mixed. The mixture was heated to 150° C., the pressure was raised to 10 bars and the mixture was stirred overnight. The mixture was then cooled down to room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07842829B2 |
|---|
| Source dataset | uspto-grants-2010_11 |
|---|
| ORD ID | ord-4709d9aeb27444bc92a958a20f0f5c21 |
|---|
| Source note | uspto-grants-2010_11 |
|---|
