HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-hydroxy-2-methylbenzofuran-6-carboxylate → Ethyl 4-({6-[(dimethylamino)carbonyl]-1-oxidopyridin-3-yl}oxy)-2-methyl-1-benzofuran-6-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-hydroxy-2-methylbenzofuran-6-carboxylate | HCID 11514065 | — |
| Reactant | 5-Bromo-N,N-dimethylpyridine-2-carboxamide 1-oxide | HCID 59560039 | — |
| Product | Ethyl 4-({6-[(dimethylamino)carbonyl]-1-oxidopyridin-3-yl}oxy)-2-methyl-1-benzofuran-6-carboxylate | HCID 59560221 | — |
Reaction Steps
The title compound was synthesized in a similar fashion as described for Intermediate 252d, by reacting ethyl 4-hydroxy-2-methylbenzofuran-6-carboxylate and 5-bromo-N,N-dimethylpyridine-2-carboxamide 1-oxide. LC-MS (ESI, pos): 386.00.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07842713B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-69306ab28410418ab8bdf02081e33962 |
| Source note | uspto-grants-2010_11 |