Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Zinc Sulfate | HCID 24424 | — |
| Edukt | Ferrous oxide | HCID 449809 | — |
| Edukt | Aluminum(III) Chloride | HCID 6451240 | — |
| Edukt | Potassium Lactate | HCID 23671663 | — |
| Edukt | Disodium myristoyl glutamate | HCID 71587140 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | Ferrous oxide | HCID 449809 | — |
| Produkt | Zinc Lactate | HCID 3007856 | — |
| Produkt | Tris(N-(1-oxotetradecyl)-L-glutamato(2-))dialuminium | HCID 56843224 | — |
Reaktionsschritte
One hundred grams of red iron oxide pigment was added to 500 ml of water and mixed using a home type mixer until well dispersed. Four grams of sodium N-myristoyl-L-glutamate having an HLB value of 4 was dissolved in 50 ml of water heated at 60° C. then added to the above mixture and mixed for 10 minutes. While this was being stirred, 2 chemical equivalents of aluminum chloride aqueous solution, based on the sodium N-myristoyl-L-glutamate, was added dropwise. Four grams of potassium lactate having an HLB value of 17 was dissolved in 50 ml of water heated at 50° C. then added to the above mixture and mixed for 10 minutes. While this was being stirred, 2 chemical equivalents of zinc sulfate aqueous solution, based on the potassium lactate, was added dropwise. The product was filtered with suction using a Buchner funnel, followed by rinsing with purified water. The filter cake was then baked in an oven for two hours after the filter cake reaches a temperature of 100° C. to further dehydrate the filter cake. The cake was crushed and pulverized to a powder after cooling. This resulted in a red iron oxide pigment chemically immobilized with aluminum N-myristoyl-L-glutamate and zinc lactate.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US07276113B2 |
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| Quelldatensatz | uspto-grants-2007_10 |
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| ORD ID | ord-6a8c24ac6a7e4d08b0674a65affce1f6 |
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| Quellennotiz | uspto-grants-2007_10 |
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