2-Morpholinoethanol → HCID 58932077, compound

HRID 1178180Notes

Reaction equation

HRID 1178180 reaction equation
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][OH:9])[CH2:3][CH2:2]1.[C:10]1([C:20](Cl)=[O:21])[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]=[CH:12][CH:11]=1>>[C:10]1([C:20]([O:9][CH2:8][CH2:7][N:4]2[CH2:5][CH2:6][O:1][CH2:2][CH2:3]2)=[O:21])[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]=[CH:12][CH:11]=1

Participants

3

Reactant 2

HCID 611632-MorpholinoethanolHCID 701461-Naphthalenecarbonyl chloride

Product 1

HCID 58932077HCID 58932077, compoundYield 94%

Procedure

The procedure of Synthesis Example 1 was repeated except that 2-morpholinoethanol was used instead of the triethanolamine, and 1-naphthoyl chloride was used instead of the benzoyl chloride, to give 2-morpholinoethyl 1-naphthalenecarboxylate in a yield of 94%.

Workup

  1. customThe procedure of Synthesis Example 1

Sources & evidence

ORD record
ord-91b02176b78b49d5b52c0f8a167644b2
Source dataset
uspto-grants-2007_10
Patent number
US07276324B2

Reaction notes

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