2-Morpholinoethanol → HCID 58974442, compound

HRID 1178181Notes

Reaction equation

[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][OH:9])[CH2:3][CH2:2]1.[CH:10]1[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]=[CH:12][C:11]=1[C:20](Cl)=[O:21]>>[CH:10]1[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]=[CH:12][C:11]=1[C:20]([O:9][CH2:8][CH2:7][N:4]1[CH2:5][CH2:6][O:1][CH2:2][CH2:3]1)=[O:21]

Participants

Reactant 2

HCID 611632-Morpholinoethanol

HCID 752462-Naphthoyl chloride

Product 1

HCID 58974442HCID 58974442, compoundYield 95%

Procedure

The procedure of Synthesis Example 1 was repeated except that 2-morpholinoethanol was used instead of the triethanolamine, and 2-naphthoyl chloride was used instead of the benzoyl chloride, to give 2-morpholinoethyl 2-naphthalenecarboxylate in a yield of 95%.

Workup

customThe procedure of Synthesis Example 1

Sources & evidence

ORD record: ord-3f51572fa0854f66918e0302d48701d8
Source dataset: uspto-grants-2007_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07276324B2

Reaction notes

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