2-Morpholinoethanol → HCID 58974428, compound

HRID 1178182Notes

Reaction equation

[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][OH:9])[CH2:3][CH2:2]1.[C:10]1([C:16]2[CH:24]=[CH:23][C:19]([C:20](Cl)=[O:21])=[CH:18][CH:17]=2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[C:10]1([C:16]2[CH:17]=[CH:18][C:19]([C:20]([O:9][CH2:8][CH2:7][N:4]3[CH2:5][CH2:6][O:1][CH2:2][CH2:3]3)=[O:21])=[CH:23][CH:24]=2)[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=1

Participants

Reactant 2

HCID 611632-Morpholinoethanol

HCID 841514-Phenylbenzoyl chloride

Product 1

HCID 58974428HCID 58974428, compoundYield 93%

Procedure

The procedure of Synthesis Example 1 was repeated except that 2-morpholinoethanol was used instead of the triethanolamine, and 4-phenylbenzoyl chloride was used instead of the benzoyl chloride, to give 2-morpholinoethyl 4-phenylbenzoate in a yield of 93%.

Workup

customThe procedure of Synthesis Example 1

Sources & evidence

ORD record: ord-2c223fefb7074d8eb34fda418bec8dd5
Source dataset: uspto-grants-2007_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07276324B2

Reaction notes

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