4-(5-chloro-[1H]-indol-3-yl)-piperidine → HCID 131724869, compound

Participants

Role	Name	HCID	Charge
Reactant	4-(5-chloro-[1H]-indol-3-yl)-piperidine	HCID 12831375	—
Reactant	1-(4-Bromobutan-1-yl)-3,4-dihydroquinolin-2(1H)-one	HCID 12992368	—
Product	HCID 131724869	HCID 131724869	—

Reaction Steps

from 5-chloro-3-(piperidin-4-yl)-1H-indole and 1-(4-bromobutan-1-yl)-3,4-dihydroquinolin-2(1h)-one. Mp 229-231° C. 1H NMR (DMSO-d6): 1.55-1.65 (m, 2H); 1.70-1.80 (m, 2H); 2.00-2.15 (m, 4H); 2.55 (t, 2H); 2.85 (t, 2H); 2.95-3.15 (m, 5H); 2.55 (d, 2H); 3.95 (t, 2H); 7.00 (t, 1H); 7.05 (d, 1H); 7.15 (d, 1H); 7.20-7.30 (m, 3H); 7.40 (d, 1H); 7.75 (s, 1H); 10.05 (broad s, 1H); 11.10 (s, 1H). MS m/z: 436 (MH+).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07276508B2
Source dataset	uspto-grants-2007_10
ORD ID	ord-f7f22af6def449b09127643900bb109a
Source note	uspto-grants-2007_10