Indole → HCID 68492239, compound

Participants

Reaction Steps

[6-(1H-Indol-3-yl)-6H-phenanthridin-5-yl]-phenyl-methanone was prepared from phenanthridine, benzoyl chloride, and indole according to GP 2. Yield, 11%. 1H-NMR (DMSO-d6): δ=6.20 (dd, J=2.5 Hz, J=0.8 Hz, 1H), 6.36 (s, br., 1H), 6,80 (t, J=7.6 Hz, 1H), 6.99-7.08 (m, 2H), 7.11 (ddd, J=J=7.5 Hz, J=1.2 Hz, 1H), 7.19-7.31 (m, 6H), 7.37 (“t”, J≈7.1 Hz, 1H), 7.43 (“t”, J≈7 Hz, 1H), 7.54 (“t”, J≈7 Hz, 2H), 7.85-7.90 (m, 1H), 7.95 (dd, J=7.8 Hz, J=1.2 Hz, 1H), 8.10 (“d”, J≈7.5 Hz, 1H), 10.69 (s, 1H); (+)-ESI-MS: m/z=401 [M+H]+, 284 [M-indole+H]+.

Provenance & Evidence