Indole → HCID 69423619, compound

Participants

Reaction Steps

[6-(1H-Indol-3-yl)-6H-phenanthridin-5-yl]-(3-methoxy-phenyl)-methanone was prepared from phenanthridine, 3-methoxybenzoyl chloride, and indole according to GP 2. Yield, 84%. 1H-NMR (CD3OD): δ=3.62 (s, 3H), 6.19 (s, 1H), 6.37 (s, br., 1H), 6.71-6.86 (m, 3H), 6.91 (dd, J=8.1 Hz, J=1.9 Hz, 1H), 7.02-7.26 (m, 5H), 7.32 (s, br., 1H), 7.39-7.48 (m, 2H), 7.54 (td, J=7.1 Hz, J=2.5 Hz, 1H), 7.90 (dd, J=7.9 Hz, J=1.2 Hz, 1H), 7.97 (s, br., 1H), 8.06 (d, J=7.8 Hz, 1H); (+)-ESI-MS: m/z=431 [M+H]+, 314 [M-indole+H]+.

Provenance & Evidence