HCID 58975531, compound → HCID 11751853, compound

Participants

Reaction Steps

The title compound (6 mg) was prepared from 12A (14.5 mg, somewhat impure) according to the procedures described in 3D and 3E. HPLC/MS retention time=3.9 min (Phenomenex Luna 5 micron C18 4.6 mm×50 mm column eluted with a 0% to 100% B solvent gradient over 4 min; solvent A=90% H2O, 10% MeOH, 10 mM NH4OAc and solvent B=10% H2O, 90% MeOH, 10 mM NH4OAc; flow rate=4.0 mL/min; UV detection at 220 nm); m/z=475 [M+H]+.

Provenance & Evidence