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HRID1178910

反应详情

EQUATION

反应方程式

HRID 1178910 的结构方程式

REACTANTS

反应物

3
结构：CCCC[N+](CCCC)(CCCC)CCCC.[F-]
HCID2724141

Tetra-n-butylammonium fluoride

C16H36FN

结构：c1ccc2c(N3CCOCC3)c[nH]c2c1
HCID12530833

未命名化合物

结构：CC(C)[Si](C(C)C)(C(C)C)n1cc(N2CCN(C)CC2)c2ccccc21
HCID58975109

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCN(c2c[nH]c3ccccc23)CC1
HCID53414691

3-(4-Methylpiperazin-1-yl)-1H-indole

C13H17N3

PROCEDURE

实验过程

Following a method similar to 3-morpholin-4-yl-1H-indole using 3-(4-Methyl-piperazin-1-yl)-1-triisopropylsilanyl-1H-indole (0.35 g, 0.94 mmol) and 1N solution of tetrabutylammonium fluoride (1.40 mL) to prepare the title compound. Purify by flash chromatography using 2 to 12% methanol in dichloromethane to give the title compound (0.12 g 60%). MS (ES) 216.1 (M+1)+.