Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Cyclopentyl(2-fluorophenyl)methanone | HCID 13771614 | — |
| Product | HCID 178419918 | HCID 178419918 | 89% |
Reaction Steps
Dissolve Cyclopentyl-(2-fluoro-phenyl)-methanone (2.5 g 13.005 mmoles) in hydrazine (20 ml) heat to 130° C. for 72 hrs. Cool mixture to 0° C. Filter the precipitate and wash with cold water to give the title compound: 2.171 g (yield=89%) MS ES+ 187.12:MSES− 185.22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07276516B2 |
|---|
| Source dataset | uspto-grants-2007_10 |
|---|
| ORD ID | ord-3b67863e64f04e98a7adad03a2d885f7 |
|---|
| Source note | uspto-grants-2007_10 |
|---|
