HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → AGN-PC-0NHP1N
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 2-Ethyl-4,7-benzoxazoledione | HCID 12071590 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | AGN-PC-0NHP1N | HCID 12071587 | — |
Reaction Steps
A mixture of 2-ethyl-1,3-benzoxazole-4,7-dione (1 eq) and aniline (1.1 eq.) in ethanol is kept under stirring for 1 hour. The reaction medium turns to dark violet. After concentration, the residue is purified by medium pressure chromatography on silica in order to produce a violet-coloured powder. Melting point: 200° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07279467B2 |
| Source dataset | uspto-grants-2007_10 |
| ORD ID | ord-ab2e556f5bf34a2cb0e8e96933e82ae2 |
| Source note | uspto-grants-2007_10 |