2-(3-Bromophenyl)ethan-1-ol → Benzeneethanol, 3-bromo-, 1-methanesulfonate

HRID 1179531Notes

Reaction equation

HRID 1179531 reaction equation
[CH3:1][S:2]([O:5][CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([N+]([O-])=O)[CH:9]=1)(=[O:4])=[O:3].[Br:17]C1C=C(CCO)C=CC=1>>[CH3:1][S:2]([O:5][CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([Br:17])[CH:9]=1)(=[O:4])=[O:3]

Participants

3

Reactant 2

HCID 27340902-(3-Bromophenyl)ethan-1-olHCID 219738843-Nitrophenethyl methanesulfonate

Product 1

HCID 57444273Benzeneethanol, 3-bromo-, 1-methanesulfonateYield 77%

Procedure

The title compound was prepared in 77% yield using a similar procedure to description D4 starting from 2-(3-bromophenyl)ethanol.

Sources & evidence

ORD record
ord-87c9a193199e465b98dde7bdfc7df08f
Source dataset
uspto-grants-2007_10
Patent number
US07279481B2

Reaction notes

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