Formic Acid → HCID 178516277, compound

HRID 1179682Notes

Reaction equation

HRID 1179682 reaction equation
Cl[C:2]1[N:3]=[N:4][C:5]([O:8][C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[C:11]([Cl:16])[CH:10]=2)=[CH:6][CH:7]=1.C(O)=[O:18]>>[Cl:16][C:11]1[CH:10]=[C:9]([CH:14]=[CH:13][C:12]=1[Cl:15])[O:8][C:5]1[N:4]=[N:3][C:2]([OH:18])=[CH:7][CH:6]=1

Participants

3

Reactant 2

HCID 284Formic AcidHCID 22047707HCID 22047707, compound

Product 1

HCID 178516277HCID 178516277, compound

Procedure

A solution of 3-chloro-6-(3,4-dichloro-phenoxy)-pyridazine (1.74 g, 6.32 mmol) in formic acid (25 mL) was heated at 100° C. for 3 hours. The solvent was removed by evaporation in vacuo yielding the title compound, which was used without further purification.

Workup

  1. customThe solvent was removed by evaporation in vacuo

Sources & evidence

ORD record
ord-f3572a50f8ef4bf5b7b040052ad38f29
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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