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HRID1179701

反应详情

EQUATION

反应方程式

HRID 1179701 的结构方程式

REACTANTS

反应物

2
结构：CN(C(=O)Cl)c1ccccc1
HCID77969

Carbamic chloride, methylphenyl-

C8H8ClNO

结构：Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1
HCID155241

4-[[5-(Trifluoromethyl)-2-pyridinyl]oxy]phenol

C12H8F3NO2

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(Oc2ccc(C(F)(F)F)cn2)cc1)c1ccccc1
HCID10150601

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was purified by preparative HPLC (36%, white crystals). HPLC-MS m/z=389.1 (M+1), Rt: 5.13 min.

WORKUP

后处理

  1. customThe crude product was purified by preparative HPLC (36%, white crystals)