Carbamic chloride, N-methyl-N-phenyl- → HCID 10150622, compound

HRID 1179705Notes

Reaction equation

HRID 1179705 reaction equation
[Cl:1][C:2]1[CH:3]=[N:4][CH:5]=[C:6]([Cl:16])[C:7]=1[O:8][C:9]1[CH:14]=[CH:13][C:12]([OH:15])=[CH:11][CH:10]=1.[CH3:17][N:18]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:19](Cl)=[O:20]>>[Cl:16][C:6]1[CH:5]=[N:4][CH:3]=[C:2]([Cl:1])[C:7]=1[O:8][C:9]1[CH:10]=[CH:11][C:12]([O:15][C:19](=[O:20])[N:18]([CH3:17])[C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[CH:13][CH:14]=1

Participants

3

Reactant 2

HCID 77969Carbamic chloride, N-methyl-N-phenyl-HCID 27265874-[(3,5-Dichloro-4-pyridinyl)oxy]phenol

Product 1

HCID 10150622HCID 10150622, compound

Procedure

The title compound was prepared from 4-(3,5-dichloro-pyridine-4-yloxy)-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was purified by preparative HPLC (41%, white crystals). HPLC-MS m/z=389.1 (M+1), Rt: 4.97 min.

Workup

  1. customThe crude product was purified by preparative HPLC (41%, white crystals)

Sources & evidence

ORD record
ord-40630ecaf18043a3a78e8bcb74dd70b9
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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