4-Butoxyphenol → HCID 10286290, compound

HRID 1179725Notes

Reaction equation

HRID 1179725 reaction equation
[CH2:1]([O:5][C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH3:4].[CH3:13][N:14]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[C:15](Cl)=[O:16]>>[CH2:1]([O:5][C:6]1[CH:7]=[CH:8][C:9]([O:12][C:15](=[O:16])[N:14]([CH3:13])[C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)=[CH:10][CH:11]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 312334-ButoxyphenolHCID 77969Carbamic chloride, N-methyl-N-phenyl-

Product 1

HCID 10286290HCID 10286290, compound

Procedure

The title compound was prepared from 4-butoxy-phenol and N-methyl-N-phenylcarbamoyl chloride. The crude product was recrystallized from ethanol (22%, white crystals). HPLC-MS m/z=300.1 (M+1), Rt: 5.20.

Workup

  1. customThe crude product was recrystallized from ethanol (22%, white crystals)

Sources & evidence

ORD record
ord-5c77702a1ace435193a393cae42830c4
Source dataset
uspto-grants-2007_10
Patent number
US07279470B2

Reaction notes

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