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HRID1179727

反应详情

EQUATION

反应方程式

HRID 1179727 的结构方程式

REACTANTS

反应物

3
结构：O=P([O-])([O-])[O-]
HCID1061

Phosphate

O4P-3

结构：CN(C(=O)Cl)c1ccccc1
HCID77969

Carbamic chloride, methylphenyl-

C8H8ClNO

结构：Oc1ccc(-c2nc(CCl)cs2)cc1
HCID605504

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(-c2nc(CCl)cs2)cc1)c1ccccc1
HCID10172371

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-(4-chloromethyl-thiazol-2-yl)-phenol and N-methyl-N-phenylcarbamoyl chloride. The aqueous phase was adjusted to PH 7.0 (phosphate buffer), before extraction with ethyl acetate. The crude product was subjected to preparative HPLC (21%, white crystals). HPLC-MS m/z=359.0 (M+1), Rt: 4.60.

WORKUP

后处理

  1. extractionbefore extraction with ethyl acetate